|
TYPE / NAME OF THE STUDY |
GUIDELINES |
| 5-BATCH
ANALYSIS |
EPA,
OPPTS |
OECD |
EEC |
CIPAC |
|
5 batch
analysis |
830.1700 |
- |
- |
- |
|
|
|
|
|
| PHYS-CHEM
ANALYSIS |
EPA,
OPPTS |
OECD |
EEC |
CIPAC |
|
Characterization of Active (Certificate of
Analysis) |
- |
- |
- |
- |
|
Appearance- Physical state |
830.6303 |
- |
- |
- |
|
Appearance- Colour |
830.6302 |
- |
- |
- |
|
Appearance- Odour |
830.6302 |
- |
- |
- |
|
Method Development and Validation (A.I.
content) |
SANCO
3030/99/830.1800 |
- |
- |
- |
|
Acidity / Alkalinity / pH |
830.7000 |
- |
- |
MT - 31/MT-75 |
|
Boiling point/Boiling range- Dynamic |
830.7220 |
103 |
A.2 |
- |
|
Characterisation (a.i., NMR / MS / IR / UV) |
- |
- |
- |
- |
|
Corrosion characteristics |
830.6320 |
- |
- |
- |
|
Density / specific gravity |
830.7300 |
109 |
A.3 |
MT - 3 |
|
Flammability - Liquid |
830.6315 |
- |
- |
MT - 12 |
|
Flammability - Solid |
830.6315 |
- |
A.10 |
MT - 12 |
|
Flash point |
830.6315 |
- |
A.9 |
MT - 12 |
|
IR / FTIR spectra |
- |
- |
- |
- |
|
Melting point/Melting range/Freezing
Temperature-Capillary Tube |
830.7200 |
102 |
A.1 |
MT-1/MT-2 |
|
Miscibility (hydrocarbon oil) |
830.6319 |
- |
- |
MT - 23 |
|
Moisture content |
- |
- |
- |
MT - 32 |
|
MS Spectra |
- |
- |
- |
- |
|
NMR spectra |
- |
- |
- |
- |
|
Oxidation / reduction |
830.6314 |
- |
- |
- |
|
Oxidizing properties (Solid) |
- |
- |
A.17 |
- |
|
Partition coefficient (Octanol: water) -
Shake flask method |
830.7550 |
107 |
A.8 |
- |
|
Partition coefficient (Octanol: water) -
HPLC Method |
830.7570 |
117 |
A.8 |
- |
|
Reaction with packaging material |
830.6317 |
- |
- |
- |
|
Auto self ignition (Solid) / Auto
Flammability |
- |
- |
A.15 |
- |
|
Shelf life (storage stability)- 1 year / 2
Year / 5 Year |
830.6317 |
- |
- |
- |
|
Solvent solubility |
830.7840 |
105 |
A.6 |
- |
|
Storage Stability- Cold temperature (0 to
-20°C) |
830.6317 |
- |
- |
- |
|
Storage Stability- Heat stability (54 ±
2°C) |
830.6317 |
- |
- |
MT - 46 |
|
Storage Stability- With metal and metal iron
at elevated temperature |
830.6313 |
- |
- |
- |
|
Storage Stability- Air stability/Thermal
stability each |
- |
113 |
- |
- |
|
Surface tension (Liquids / Solid) |
- |
115 |
A.5 |
- |
|
UV/Vis absorption |
830.7050 |
101 |
- |
- |
|
Vapour pressure |
830.7950 |
104 |
A.4 |
- |
|
Viscosity of liquids |
830.7100 |
114 |
- |
MT - 22 |
|
Water solubility (3 pH) - Shake flask method |
830.7840 |
105 |
A.6 |
- |
|
Water solubility (3 pH) - Column method |
830.7860 |
105 |
A.6 |
- |
|
|
|
|
|
| FORMULATION
PRODUCT |
EPA,
OPPTS |
OECD |
EEC |
CIPAC |
|
Dry Sieve Test |
- |
- |
- |
MT 59.1 |
|
Dustability |
- |
- |
- |
MT 34 |
|
Dispersive characteristics |
- |
- |
- |
MT - 180/36.1 |
|
Form Persistence |
- |
- |
- |
MT - 47.2 |
|
Low Temperature Stability |
- |
- |
- |
MT - 39.1 |
|
Pourability
|
- |
- |
- |
MT - 148 |
|
Wet Sieve Test |
- |
- |
- |
MT - 59.3 |
|
Dilusion stability |
- |
- |
- |
MT - 41 |
|
Dissolution of water soluble bags |
- |
- |
- |
MT - 176 |
|
Dust Content |
- |
- |
- |
MT - 171 |
|
Flowability
|
- |
- |
- |
MT - 172 |
|
Friability and Attrition
|
- |
- |
- |
MT - 178 |
|
Degree of dispersive
|
- |
- |
- |
MT - 169 |
|
Wettability
|
- |
- |
- |
MT - 53.3 |
|
Particle size distribution
|
- |
- |
- |
MT - 58.2 |
|
Suspensibility
|
- |
- |
- |
MT - 15.1 |
|
Emulsification / Re-emulsification
|
- |
- |
- |
- |
|
Spontanity of dispersibility
|
- |
- |
- |
MT - 160 |
|
Nitrosomanine
|
- |
- |
- |
TEA |
|
|
|
|
|
|
